Determination of personal care products and hormones in leachate and groundwater from Polish MSW landfills by ultrasound-assisted emulsification microextraction and GC-MS
PBN-AR
Instytucja
Wydział Biologiczno-Chemiczny (Uniwersytet w Białymstoku)
Informacje podstawowe
Główny język publikacji
angielski
Czasopismo
Environmental Science and Pollution Research International
ISSN
0944-1344
EISSN
1614-7499
Wydawca
DOI
URL
Rok publikacji
2016
Numer zeszytu
2
Strony od-do
1642-1652
Numer tomu
23
Identyfikator DOI
Liczba arkuszy
1,6
Słowa kluczowe
angielski
Endocrine disrupting compounds; Gas chromatography–mass spectrometry; Groundwater; Hormones; Landfill leachate; Personal care products; Ultrasound-assisted emulsification microextraction
Streszczenia
Język
angielski
Treść
Determination of the endocrine disrupting compounds (EDCs) in leachate and groundwater samples from the landfill sites is very important because of the proven harmful effects of these compounds on human and animal organisms. A method combining ultrasound-assisted emulsification microextraction (USAEME) and gas chromatography-mass spectrometry (GC-MS) was developed for simultaneous determination of seven personal care products (PCPs): methylparaben (MP), ethylparaben (EP), propylparaben (PP), buthylparaben (BP), benzophenone (BPh), 3-(4-methylbenzylidene)camphor (4-MBC), N,N-diethyltoluamide (DEET), and two hormones: estrone (E1) and β-estradiol (E2) in landfill leachate and groundwater samples. The limit of detection (LOD)/limit of quantification (LOQ) values in landfill leachate and groundwater samples were in the range of 0.003-0.083/0.009-0.277 μg L(-1) and 0.001-0.015/0.002-0.049 μg L(-1), respectively. Quantitative recoveries and satisfactory precision were obtained. All studied compounds were found in the landfill leachates from Polish municipal solid waste (MSW) landfills; the concentrations were between 0.66 and 202.42 μg L(-1). The concentration of pollutants in groundwater samples was generally below 0.1 μg L(-1).
Cechy publikacji
publikacja naukowa oryginalna
Inne
System-identifier
PX-578835bcc2dc0c625e1cf2f9
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